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Beilstein J. Org. Chem. 2018, 14, 373–380, doi:10.3762/bjoc.14.25
Graphical Abstract
Scheme 1: Silicon-mediated Mukaiyama-type aldol reaction of octyl 2-(pentafluoro-λ6-sulfanyl)acetate (1) with ...
Figure 1: Newman projections of the syn- and the anti-diastereomeric aldol addition products.
Scheme 2: Mechanism of the formation of aldol addition products.
Scheme 3: Formation of (E)-configured aldol condensation products.
Scheme 4: Anticipated mechanism of formation of aldol condensation products.
Scheme 5: Synthesis of SF5-substituted acetmorpholide 8.
Scheme 6: Intermediate formation of the (Z)-ketene aminal from morpholide 8 with TMSOTf/ Et3N and subsequent ...